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Shobu, Takahisa; Shiro, Ayumi*; Yoshida, Yutaka*
Zairyo, 69(4), p.343 - 347, 2020/04
Dislocation density is a very important physical quantity in the evaluation of fatigue of metallic materials. Generally, the dislocation density is evaluated by a scanning electron microscope. Recently, a method generated the dislocation density from the width of the X-ray diffraction profile has been proposed. In this study, we report the application of this technology to synchrotron radiation. Five diffraction profiles were obtained with a two-dimensional detector during tensile loading of the austenitic stainless steel SUS316L, and the dislocation density was calculated from the line profile analysis. As a result, the dislocation density increased sharply after plastic deformation, and the value was in good agreement with the result separately measured with a scanning electron microscope. In the future, it is expected that the line profile analysis will contribute to the elucidation of the mechanism of fatigue fracture by measuring the dislocation density from the local area in materials.
Tomota, Yo*; Sato, Shigeo*; Harjo, S.
Tetsu To Hagane, 103(2), p.73 - 85, 2017/01
Times Cited Count：18 Percentile：62.47(Metallurgy & Metallurgical Engineering)Sato, Shigeo*; Onuki, Yusuke*; Shobu, Takahisa; Shiro, Ayumi*; Tashiro, Hitoshi*; Todoroki, Hidekazu*; Suzuki, Shigeru*
Kinzoku, 86(8), p.654 - 660, 2016/08
no abstracts in English
Kumagai, Masayoshi*; Akita, Koichi; Imafuku, Muneyuki*; Oya, Shinichi*
Advanced Materials Research, 996, p.39 - 44, 2014/08
Times Cited Count：6 Percentile：93.33(Engineering, Mechanical)The microstructural features of shot and laser peened austenitic stainless steels were studied using line profile analysis with X-rays. Although both specimens had similar residual stress profiles toward the depth direction, the microstructural features were different not only on the original surfaces of the specimens but also to several micrometers in depth. The dislocation densities of the SP specimen were greater than that of the LP specimen. And the crystallite sizes of the SP specimen were smaller than that of the LP specimen.
Shobu, Takahisa; Shiro, Ayumi*
no journal, ,
no abstracts in English
Shobu, Takahisa; Yasuda, Ryo*; Shiro, Ayumi*; Yoshida, Yutaka*; Tokuda, Susumu*; Shibano, Junichi*; Kumagai, Masayoshi*
no journal, ,
A dislocation density increases and fatigue failure of the structure occur, when a metal is deformed. In this study, dislocation density of a broken 0.3 mm thick SUS316L specimen was calculated by line profile analysis obtained by high energy synchrotron X-ray diffraction method, and a relationship between fatigue fracture and dislocation density was evaluated. As a result of the analysis, it was revealed that the dislocation density abruptly increases as approaching the fracture part. In addition, it was revealed that the bcc structure appeared in the fcc structure which is the basic structure in the fracture part. In steel, the increase in dislocation density is closely related to the increase in material strength, and the material strength of steel with bcc structure is known to be higher than that with fcc structure. So, it seems that the structure has changed due to a sharp increase in dislocation density at the fracture part.
